Design of the SPring-8 JAEA beamline BL22XU

Shiwaku, Hideaki; Marushita, Motoharu*

JAEA-Research 2022-015, 39 Pages, 2023/05

JAEA-Research-2022-015.pdf:2.74MB

We designed the hard X-ray undulator beamline BL22XU, which is dedicated to Japan Atomic Energy Research Institute (JAERI) at SPring-8 (now Japan Atomic Energy Agency (JAEA)). BL22XU is used for XAFS (X-ray Absorption Fine Structure) analysis experiments to develop separation and extraction materials for radioactive waste treatment and to elucidate their chemical behavior, magnetic research experiments using a diffractometer, and experiments under extreme conditions using a high-pressure press and a diamond anvil cell. The available X-ray energy range was set from 3 to 70 keV. To design the optics of the beamline, the reflectivity of the mirrors, the diffraction width of the monochromatic crystal, and the absorptance of the Be window were calculated. In addition, ray tracing was performed to optimize the materials for optics, dimensions, and location. The delay time of the ADL (Acoustic Delay Line) was also examined to ensure the safety in the use of radioactive materials. The operation of BL22XU "JAEA Actinide Science I" has already started. By collaborating BL22XU and BL23SU "JAEA Actinide Science II," which uses a soft X-ray undulator as a light source, we solve the problems to promote nuclear sciences. Since the monochromator was upgraded in 2018-2019, initial planning and measured data are documented here again.

Actual stress analysis of small-bore butt-welded pipe by complementary use of synchrotron X-rays and neutrons

Suzuki, Kenji*; Miura, Yasufumi*; Shiro, Ayumi*; Toyokawa, Hidenori*; Saji, Choji*; Shobu, Takahisa; Morooka, Satoshi

Zairyo, 72(4), p.316 - 323, 2023/04

https://doi.org/10.2472/jsms.72.316

Report of the design examination and the installation work for the radiation shield at the beam injection area in the 3 GeV synchrotron

Nakanoya, Takamitsu; Kamiya, Junichiro; Yoshimoto, Masahiro; Takayanagi, Tomohiro; Tani, Norio; Kotoku, Hirofumi*; Horino, Koki*; Yanagibashi, Toru*; Takeda, Osamu*; Yamamoto, Kazami

JAEA-Technology 2021-019, 105 Pages, 2021/11

JAEA-Technology-2021-019.pdf:10.25MB

Since a user operation startup, the 3 GeV synchrotron accelerator (Rapid-Cycling Synchrotron: RCS) gradually reinforced the beam power. As a result, the surface dose rate of the apparatus located at the beam injection area of the RCS, such as the magnet, vacuum chambers, beam monitors, etc., increases year by year. The beam injection area has many apparatuses which required manual maintenance, so reducing worker's dose is a serious issue. To solve this problem, we have organized a task force for the installation of the shield. The task force has aimed to optimize the structure of the radiation shield, construct the installation procedure with due consideration of the worker's dose suppression. As the examination result of the shield design, we have decided to adopt removal shielding that could be installed quickly and easily when needed. We carried out shield installation work during the 2020 summer maintenance period. The renewal work required to install the shielding has been carried out in a under high-dose environment. For this reason, reducing the dose of workers was an important issue. So, we carefully prepared the work plan and work procedure in advance. During the work period, we implemented various dose reduction measures and managed individual dose carefully. As a result, the dose of all workers could be kept below the predetermined management value. We had installed removal shielding at the beam injection area in the 2020 summer maintenance period. We confirmed that this shield can contribute to the reduction of the dose during work near the beam injection area. It was a large-scale work to occupy the beam injection area during almost of the summer maintenance period. However, it is considered very meaningful for dose suppression in future maintenance works.

Evaluation of internal strain distribution of dissimilar laser welding using high energy X-rays

Shobu, Takahisa; Shiro, Ayumi*; Muramatsu, Toshiharu*

SPring-8/SACLA Riyo Kenkyu Seikashu (Internet), 9(5), p.318 - 323, 2021/08

https://doi.org/10.18957/rr.9.5.318

Laser welding has already been put into practical use for various metal materials because the irradiation area is very small and the control is easy. In this study, we evaluated strain, stress, deformation, etc. near the processing affected area by high-energy synchrotron radiation X-ray diffraction method, which is one of the problems of laser welding of different materials that are expected to be put into practical use. As a result of internal deformation measurement of the bonding of dissimilar materials of copper and iron, it was confirmed that the copper side with a high coefficient of linear expansion was hardly deformed, strong tensile strain on the iron side, and a plastic deformation region on the heat-affected zone. In addition, a retained austenite phase, which is thought to be caused by the mixture of copper, was observed in the plastic deformation region of iron, and further problems were clarified in the evaluation of material strength in the mixed metallic materials.

Quantifying the dislocation structures of additively manufactured Ti-6Al-4V alloys using X-ray diffraction line profile analysis

Yamanaka, Kenta*; Kuroda, Asumi*; Ito, Miyu*; Mori, Manami*; Bian, H.*; Shobu, Takahisa; Sato, Shigeo*; Chiba, Akihiko*

Additive Manufacturing, 37, p.101678_1 - 101678_12, 2021/01

https://doi.org/10.1016/j.addma.2020.101678

Development of cryogenic tensile testing apparatus for lattice strain measurement using synchrotron radiation for REBCO composite conductors

Sugano, Michinaka*; Machiya, Shutaro*; Shobu, Takahisa; Shiro, Ayumi*; Kajiwara, Kentaro*; Nakamoto, Tatsushi*

Superconductor Science and Technology, 33(8), p.085003_1 - 085003_10, 2020/08

https://doi.org/10.1088/1361-6668/ab953e

Feasibility study on application of synchrotron radiation CT imaging to alloy steel for non-destructive inspection of inclusions

Shimamura, Yoshinobu*; Matsushita, Shinya*; Fujii, Tomoyuki*; Togo, Keiichiro*; Akita, Koichi*; Shobu, Takahisa; Shiro, Ayumi*

Metals, 9(5), p.527_1 - 527_9, 2019/05

https://doi.org/10.3390/met9050527

Observation of simulated fuel debris using synchrotron radiation

Yoneda, Yasuhiro; Harada, Makoto; Takano, Masahide

Transactions of the Materials Research Society of Japan, 44(2), p.61 - 64, 2019/04

https://doi.org/10.14723/tmrsj.44.57

We performed three-dimensional observation of simulated fuel debris using Synchrotron Computed Tomography (CT). CT was used to make the inside of fuel debris clear. The CT observation provides that a clear contrast in the zirconia rich part and concrete rich part. Zirconia heavier than concrete moved to the lower part when crystals precipitate and aggregates near the bottom surface. As a result, phase separation occurs. The phase separation is caused by the difference in the composition ratio of zirconia, and can also be observed difference in crystal growth mode by composition ratio.

Tuning strain-induced -to- martensitic transformation of biomedical Co-Cr-Mo alloys by introducing parent phase lattice defects

Mori, Manami*; Yamanaka, Kenta*; Sato, Shigeo*; Tsubaki, Shinki*; Sato, Kozue*; Kumagai, Masayoshi*; Imafuku, Muneyuki*; Shobu, Takahisa; Chiba, Akihiko*

Journal of the Mechanical Behavior of Biomedical Materials, 90, p.523 - 529, 2019/02

https://doi.org/10.1016/j.jmbbm.2018.10.038

Development of CdTe pixel detectors combined with an aluminum Schottky diode sensor and photon-counting ASICs

Toyokawa, Hidenori*; Saji, Choji*; Kawase, Morihiro*; Wu, S.*; Hurukawa, Yukihito*; Kajiwara, Kentaro*; Sato, Masugu*; Hirono, Toko*; Shiro, Ayumi*; Shobu, Takahisa; et al.

Journal of Instrumentation (Internet), 12(1), p.C01044_1 - C01044_7, 2017/01

https://doi.org/10.1088/1748-0221/12/01/C01044

We have been developing CdTe pixel detectors combined with a Schottky diode sensor and photon-counting ASICs. The hybrid pixel detector was designed with a pixel size of 200 micro-meter by 200 micro-meter and an area of 19 mm by 20 mm or 38.2 mm by 40.2 mm. The photon-counting ASIC, SP8-04F10K, has a preamplifier, a shaper, 3-level window-type discriminators and a 24-bits counter in each pixel. The single-chip detector with 100 by 95 pixels successfully operated with a photon-counting mode selecting X-ray energy with the window comparator and stable operation was realized at 20C. We have performed a feasibility study for a white X-ray microbeam experiment. Laue diffraction patterns were measured during the scan of the irradiated position in a silicon steel sample. The grain boundaries were identified by using the differentials between adjacent images at each position.